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,
, Ni) et de la ségrégation chimique dans les dendrites (W, Re majoritairement) (Figure A3.1). De même, on peut déterminer les éléments chimiques, La Figure A3.1 et la Figure A3.2 présentent des cartographies WDS des éléments présents dans le CMSX-4 Plus et dans le René N5. En particulier, on peut aisément se rendre compte des éléments constituants les agrégats eutectiques
, Figure A3.1 -Cartographie WDS en niveau de gris sur du CMSX-4 Plus (état initial) pour les différents éléments (l'image pour le Mo est manquante) où les ségrégations chimiques dans les dendrites et les agrégats eutectiques sont visibles
2 -Cartographie WDS en niveau de gris sur du René N5 (état initial) pour les différents éléments où des carbures sont visibles ,
, La Figure A4.1 présente la distribution de taille des précipités ?' pour le CMSX-4 et le CMSX-4 Plus déterminée par analyse d'image, avec un fit par une loi normale, La Figure A4.1 superpose les distributions pour l'état initial et l'état optimisé
, La taille moyenne des précipités ?' après le traitement optimisé devient presque identique si comparée entre les coeurs dendrites et les espaces interdendritiques respectivement pour chaque alliage. On peut aussi remarquer une diminution de la taille moyenne et une diminution de la largeur de la distribution des précipités ?' entre l'état initial et l'état optimisé. On peut donc confirmer que l'état optimisé présente une distribution plus homogène, Une grande disparité de taille des précipités ?' entre les coeurs de dendrites et les espaces interdendritiques pour les deux alliages dans l'état initial est observée
1 -Distributions de la taille des précipités ?' avec un fit par une loi normale dans les coeurs de dendrites (D, trait plein) et dans les espaces interdendritique (EI, trait en pointillés) pour les états de traitement thermique initial (ini) et optimisé (opti) pour : (a) le CMSX-4 ,
, Cas du CMSX-4 Plus par deux fondeurs différents
, On peut cependant noter, que la taille moyenne des précipités ?' dans l'alliage élaboré par le fondeur A est légèrement supérieure à la taille moyenne des précipités dans l'alliage élaboré par le fondeur B, dans les coeurs dendrites et dans les espaces interdendritiques. De même, La Figure A4.2 présente la distribution de taille des précipités ?' déterminée par analyse d'image
, Annexes