3 a démontré que le facteur temps avait une influence sur l'adsorption du MBT sur les surfaces d'aluminium. Ainsi, dans le cas de cette étude des temps d'immersion plus longs ont été étudiés. Des échantillons d'aluminium polis ont été immergés entre 1h et 14j dans une solution de NaCl 0,05 mol/L contenant 1,0 mmol/L de MBT, Ces échantillons ont été comparés à des échantillons de référence immergés dans NaCl sans MBT. -Aluminium, p.2 ,
, 27 montre que ces derniers sont généralement constitués de deux pics : le pic à plus faible énergie de liaison (comprise entre 73,0 et 73,1 eV) correspond à l'aluminium métallique Al (0) [132] [133] et le second pic à plus haute énergie de liaison, La décomposition détaillée des spectres Al2p présentée en figure 4
,
, cela signifie que l'épaisseur de l'oxyde formé en surface est trop importante pour que le métal soit détecté. Pour rappel, on estime que 95% du signal XPS provient des photoélectrons situés à une profondeur inférieure à trois fois leur libre parcours moyen soit environ 10 nm. En supposant que la couche d'oxyde formée est uniforme et continue, il est alors possible d'appliquer l'équation 2.15 décrite au chapitre 2 pour déterminer son épaisseur. Les résultats présentés dans le tableau 4.9 montrent que pour des temps d'immersion supérieurs à 1h, l'ajout de MBT entraine une diminution de l'épaisseur de la couche d'oxyde
Effet inhibiteur du 2-mercaptobenzothiazole et du 2-mercaptobenzimidazole sur la corrosion du cuivre et de l'aluminium ,
, Décomposition des spectres du niveau de coeur S2p des échantillons d'aluminium immergés dans NaCl 0,05 mol/L a) 1h, a') 1h avec MBT, b) 24h, b') 24h avec MBT, c) 72h, c') 72h avec MBT, d) 14j, d') 14j avec MBT, vol.30
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