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, On n'observe que les bandes caractéristiques du PE : -2915 et 2847 cm -1 : CH2 stretching antisymétrique et symétrique. -1472 et 1462 cm -1 : CH2 bending antisymétrique et symétrique. -729 et 719 cm -1 : CH2 rocking antisymétrique et symétrique, 2002.
, 11 mmol) a été dissoute dans du DMF (100 mL). La ndodecylamine (1,89 g, 10 mmol), du TBTU (4,54 g, 14 mmol) et de la DIEA (5,2 mL, 30 mmol) sont ensuite ajoutés
, x 30 mL), lavé avec de l'eau (2 x 30 mL), séché avec du sulfate de magnésium, filtré puis séché sous vide une nuit à 120°C. Une poudre blanche est obtenue. Le greffage est total d'après la 1 H RMN. -1662 cm -1 : vibration d'élongation C=O amide
,
, 10 mmol) a été dissoute dans 80 mL d'un mélange eau/éthanol (50/50 v/v). NaHCO3 (1,01 g, 12 mmol) et du 2-chloro-4,6-diaminotriazine (DAT-Cl, 1,65 g, 11 mmol) sont ajoutés et la suspension obtenue est agitée à 100°C pendant 24 heures. En fin de réaction, le milieu réactionnel est devenu transparent indiquant la réaction du DAT. Le milieu réactionnel est refroidi et le précipité obtenu est filtré
, TCE/C6D6 363 K)
3321 cm -1 : vibration d'élongation NH du DAT. -1550 cm -1 : vibrations d'élongation quadrant du cycle triazine. -1366 cm -1 : vibration de déformation C-N aromatique. -814 cm -1 : vibrations d'élongation ,
, Images en microscopie optique polarisée de DAT-PE1200-DAT à différentes températures obtenues lors du refroidissement de l'échantillon depuis 200°C à 10°C/min (échelle 100 µm)
3326 et 3187 cm -1 : vibrations NH et NH2 du DAT. -1557 cm -1 : vibrations d'élongation quadrant du cycle triazine. -1350 cm -1 : vibration de déformation C-N aromatique. -814 cm -1 : vibrations d'élongation ,
, Modélisation du trou de corrélation de Thy-PE1200-Thy et DAT-PE1200-DAT à 200°C (fThy/DAT = 0,045, N = 43) Paramètres ajustés : Rg = 21,6 Å et ?PE/Thy = 7,2 pour Thy-PE1200-Thy et Rg = 20,5 Å et ?PE/DAT = 7,1 pour DAT-PE1200-DAT
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, Peptide Nucleic Acids
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